A multi‐residue screening method for the determination of 73 pesticides and metabolites in fruit and vegetables using high‐performance liquid chromatography/tandem mass spectrometry
- 20 September 2004
- journal article
- research article
- Published by Wiley in Rapid Communications in Mass Spectrometry
- Vol. 18 (20), 2443-2450
- https://doi.org/10.1002/rcm.1645
Abstract
A multi‐residue screening method was developed for the simultaneous analysis of 73 pesticides and their metabolites using high‐performance liquid chromatography coupled with electrospray tandem mass spectrometry. These pesticides were determined under a single set of experimental conditions involving a simple acetonitrile extraction without the requirement for a clean‐up step. Validation was achieved at 0.01 and 0.1 mg kg−1 levels in apple, lettuce and orange. Recoveries were in the range 77–124% for the majority of pesticides. © Crown Copyright 2004. Reproduced with the permission of Her Majesty's Stationery Office. Published by John Wiley & Sons, Ltd.Keywords
This publication has 7 references indexed in Scilit:
- A new multi-residue method for analysis of pesticide residues in fruit and vegetables using liquid chromatography with tandem mass spectrometric detectionJournal of Chromatography A, 2003
- Applicability of Gradient Liquid Chromatography with Tandem Mass Spectrometry to the Simultaneous Screening for About 100 Pesticides in CropsJournal of AOAC INTERNATIONAL, 2003
- Fast and Easy Multiresidue Method Employing Acetonitrile Extraction/Partitioning and “Dispersive Solid-Phase Extraction” for the Determination of Pesticide Residues in ProduceJournal of AOAC INTERNATIONAL, 2003
- Pesticide Residue Analysis (1999–2000): A ReviewJournal of AOAC INTERNATIONAL, 2001
- Trace analysis of pesticides by gas chromatographyJournal of Chromatography A, 1999
- Development of a Method of Analysis for 46 Pesticides in Fruits and Vegetables by Supercritical Fluid Extraction and Gas Chromatography/Ion TVap Mass SpectrometryPublished by Oxford University Press (OUP) ,1995
- Ion Trap Detection for Development of a Multiresidue/Multi Matrix Method for Pesticide Residues in Agricultural ProductsInternational Journal of Environmental Analytical Chemistry, 1995