Determination of acrylamide in sugar by capillary GLC with alkali flame‐ionization detection
- 1 July 1989
- journal article
- research article
- Published by Taylor & Francis Ltd in Food Additives & Contaminants
- Vol. 6 (3), 377-381
- https://doi.org/10.1080/02652038909373793
Abstract
A method for the determination of acrylamide traces as a residue of anti‐incrustation agents in sugar was developed. Acrylamide was extracted into ethyl acetate after derivatization by bromination to 2,3‐dibromopropionamide (2,3‐DBPA). The extract was cleaned up on a silica gel column and analysed by gas‐liquid chromatography with an alkali flame‐ionization detector (AFID). A glass capillary column with OV‐1 stationary phase was used for this analysis. The recovery of the method determined in model experiments was 70.0% and 77.1% at 100 μG kg−1 and 20 μg kg−1, respectively. The limit of detection of acrylamide in sugar is 1–10 μg kg−1. Parameters of the described method are compared with other published methods.Keywords
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