Orthorhombicity and oxygen uptake by YBa2Cu3O6 + x

Abstract
We have measured, at different oxygen contents, the cell parameters of YBa2Cu3O6+x between 24 and 260 K using cold neutrons. The results of profile refinement of our high resolution data is shown in figure 1 ; it does not confirm the X-ray finding, recently reported [1], showing a cusp in the orthorhombic splitting b — a, around the superconducting transition temperature. It has also been evidenced that the volume of the crystallographic cell is contracted by oxygen uptake