Effect of high temperature heat treatments on the quality factor of a large-grain superconducting radio-frequency niobium cavity
Open Access
- 10 April 2013
- journal article
- research article
- Published by American Physical Society (APS) in Physical Review Special Topics - Accelerators and Beams
- Vol. 16 (4), 042001
- https://doi.org/10.1103/physrevstab.16.042001
Abstract
Large-grain Nb has become a viable alternative to fine-grain Nb for the fabrication of superconducting radio-frequency cavities. In this contribution we report the results from a heat treatment study of a large-grain 1.5 GHz single-cell cavity made of “medium purity” Nb. The baseline surface preparation prior to heat treatment consisted of standard buffered chemical polishing. The heat treatment in the range was done in a newly designed vacuum induction furnace. values of the order of at 2.0 K and peak surface magnetic field () of 90 mT were achieved reproducibly. A value of at 2.0 K and was obtained after heat treatment at . This is the highest value ever reported at this temperature, frequency, and field. Samples heat treated with the cavity at were analyzed by secondary ion mass spectrometry, x-ray photoelectron spectroscopy, energy dispersive x ray, point-contact tunneling, and x-ray diffraction, and revealed a complex surface composition which includes titanium oxide, increased carbon, and nitrogen content but reduced hydrogen concentration compared to a non-heat-treated sample.
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Funding Information
- U.S. Department of Energy
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