Synthesis of Microporous Ti-Si-O Materials from a Titanium-containing Oligosilsesquioxane

Abstract
Microporous Ti-Si mixed oxides with high surface areas were prepared by the calcination of a titanium-containing oligosilsesquioxane with a cubic core structure, [CpTi(R7Si7O12)] (R = c-C5H9) 1b, or silica-supported 1b.
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