Synthesis of nanostructured zirconium monosilicide via a lithium thermal reduction route at low temperature
- 1 December 2020
- journal article
- research article
- Published by Walter de Gruyter GmbH in International Journal of Materials Research
- Vol. 111 (12), 1047-1050
- https://doi.org/10.3139/146.111968
Abstract
In this paper, orthorhombic phase zirconium monosilicide nanomaterials have been successfully synthesized through a lithium thermal reduction in a stainless-steel autoclave at a low temperature of 600 °C. X-ray diffraction indicates that the obtained product is orthorhombic zirconium monosilicide. Scanning electron microscopy shows that the obtained zirconium monosilicide product consists of nanoparticles and nanorods. The oxidation resistance of the obtained zirconium monosilicide product is investigated.Keywords
This publication has 25 references indexed in Scilit:
- Synthesis of zirconium silicide in Zr thin film on Si and study of its surface morphologyJournal of Materials Science: Materials in Electronics, 2013
- Solid state synthesis of a new ternary nitride MgMoN2 nanosheets and micromeshesJournal of Materials Chemistry, 2012
- Nuclear-grade zirconium prepared by combining combustion synthesis with molten-salt electrorefining techniqueJournal of Nuclear Materials, 2011
- Rapid and cost-effective method for synthesizing zirconium silicidesChemical Engineering Journal, 2010
- Mechanical properties of ZrB2–SiC(ZrSi2) ceramicsJournal of the European Ceramic Society, 2010
- Synthesis and applications of metal silicidenanowiresJournal of Materials Chemistry, 2009
- Consolidation of nanostructured ZrSi2–Si3N4 synthesized from mechanically activated (4ZrN+11Si) powders by high frequency induction heated combustion synthesisMaterials Research Bulletin, 2009
- Combustion synthesis of Zr–Si intermetallic compoundsJournal of Alloys and Compounds, 1999
- X-ray diffraction study of mechanochemical synthesis and formation mechanisms of zirconium carbide and zirconium silicidesJournal of Alloys and Compounds, 1998
- Morphology of TiSi2 and ZrSi2 on Si(100) and (111) surfacesJournal of Materials Research, 1994