Simultaneous Determination of Eight Bioactive Components of Radix Dipsaci by Near-infrared Spectroscopy
- 25 September 2017
- journal article
- pharmaceutical analysis
- Published by Taylor & Francis Ltd in Analytical Letters
- Vol. 50 (16), 2634-2648
- https://doi.org/10.1080/00032719.2017.1307384
Abstract
A new method was developed using Fourier transform near-infrared spectroscopy and high-performance liquid chromatography with diode array detection for the identification and determination of eight major compounds in crude and sweated Radix Dipsaci. Partial least square regression was selected for the analysis. Multiplicative scatter correction, first derivative, and a Savitzky–Golay filter were used for the spectral pretreatment of the crude material, while standard normal variation, first derivative, and the Savitzky–Golay filter were used for the sweated samples. The correlation coefficients of the calibration models were above 0.99 and the root mean square error of calibration, the root mean square error of prediction, and root mean square error of cross-validation were under 0.63. The developed models were used to analyze unknown crude and sweated Radix Dipsaci with satisfactory results. The established methods were rapid, simple, nondestructive, and useful for quality control of Radix Dipsaci.Keywords
Funding Information
- National Natural Science Foundation of China (81303224)
- National Scientific Research of Traditional Chinese Medicine Industry, Quality guarantee system of Chinese herbal medicines (201507002)
- Public Welfare Technology Application Research Project of Zhejiang Province (2015C33152)
- Open Fund Project of First-Class Key Discipline of Zhejiang Chinese Medical University
This publication has 16 references indexed in Scilit:
- In vitro COX-1 and COX-2 enzyme inhibitory activities of iridoids from Penstemon barbatus, Castilleja tenuiflora, Cresentia alata and Vitex mollisBioorganic & Medicinal Chemistry Letters, 2015
- Simultaneous Detection of Flavonoids, Phenolic Acids and Alkaloids in Abri Herba and Abri Mollis Herba using Liquid Chromatography Tandem Mass SpectrometryPhytochemical Analysis, 2015
- Application of Cornelian Cherry Iridoid-Polyphenolic Fraction and Loganic Acid to Reduce Intraocular PressureEvidence-Based Complementary and Alternative Medicine, 2015
- High performance liquid chromatography coupled to electrospray ionization and quadrupole time-of-flight–mass spectrometry as a powerful analytical strategy for systematic analysis and improved characterization of the major bioactive constituents from Radix DipsaciJournal of Pharmaceutical and Biomedical Analysis, 2014
- Treatment of Radix Dipsaci extract prevents long bone loss induced by modeled microgravity in hindlimb unloading ratsPharmaceutical Biology, 2014
- Near-infrared Reflectance Spectroscopy as a Rapid and Non-destructive Analysis Tool for Curcuminoids in TurmericPhytochemical Analysis, 2014
- Rapid Determination of the Main Compounds in Crude and Processed Atractylodes macrocephala Using Fourier Transform Infrared Spectroscopy with Attenuated Total ReflectanceAnalytical Letters, 2014
- Quantitative determination and pattern recognition analyses of bioactive marker compounds from Dipsaci Radix by HPLCArchives of Pharmacal Research, 2013
- Application of Fourier Transform Near-Infrared Spectroscopy Combined with High-Performance Liquid Chromatography in Rapid and Simultaneous Determination of Essential Components in Crude Radix ScrophulariaeAAPS PharmSciTech, 2012
- Asperosaponin VI, A Saponin Component from Dipsacus asper Wall, induces Osteoblast Differentiation through Bone Morphogenetic Protein‐2/p38 and Extracellular Signal‐regulated Kinase 1/2 PathwayPhytotherapy Research, 2011