3-[N-(4-Methoxybenzyl)amino]benzo[de]anthracen-7-one
Open Access
- 11 October 2021
- Vol. 2021 (4), M1287
- https://doi.org/10.3390/M1287
Abstract
Herein, we describe the synthesis of 3-[N-(4-methoxybenzyl)amino]benzo[de]anthracen-7-one via a two-step procedure including 3-aminobenzanthrone condensation with anisaldehyde and following reduction of obtained imine to appropriate amine by sodium borohydride. The structure of the synthesized compounds was established by elemental analysis, nuclear magnetic resonance spectroscopy, mass spectrometry (EI-MS), and infrared spectroscopy (FT-IR) and confirmed by single-crystal X-ray diffraction. The title compound was analyzed by thermal gravimetric analysis, UV/vis, and fluorescence spectroscopy.Keywords
Funding Information
- Daugavpils University (14-89/2021/2)
This publication has 11 references indexed in Scilit:
- Benzanthrone dyes as mediators of cascade energy transfer in insulin amyloid fibrilsJournal of Molecular Liquids, 2020
- Asymmetric catalytic hydrogenation of imines and enamines in natural product synthesisGreen Synthesis and Catalysis, 2020
- A Simple and Rapid Staining Technique for Sex Determination of Trichinella Larvae Parasites by Confocal Laser Scanning MicroscopyMicroscopy and Microanalysis, 2019
- Novel dye for detection of callus embryo by confocal laser scanning fluorescence microscopyLuminescence, 2019
- Boron Hydride ReductionACS Symposium Series, 2016
- A short history of SHELXActa Crystallographica Section A Foundations of Crystallography, 2007
- Spectral Properties of 3-Benzanthrone Derivative Dyes in Isotropic Solvents, Polymer Film and Liquid CrystalZeitschrift für Naturforschung A, 2001
- Functional properties of azomethine substituted benzanthrone dyes for use in nematic liquid crystalsJournal of Molecular Structure, 1998
- Synthesis and properties of benzanthrone derivatives as luminophore dyes for liquid crystalsDyes and Pigments, 1998
- Zur Kenntnis des BenzanthronsEuropean Journal of Organic Chemistry, 1929