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Synthesis, characterization, kinetic and thermodynamic parameters evaluation from TG-DTA analysis of Cu(II), Co(II) and Mn(II) complexes with two phenol Schiff bases

Published: 31 December 2016
European Journal of Chemistry , Volume 7, pp 436-441; doi:10.5155/eurjchem.7.4.436-441.1445

Abstract: Complexes of Cu(II), Co(II) and Mn(II) with two Schiff base ligands {[(2-carboxyphenyl)imino]methyl} phenol (HLA) and {[(2-hydroxyphenyl)imino]methyl} phenol (HLB) were synthesized and characterized by FT-IR, UV-Visible, 1H NMR spectroscopy and elemental analysis. All the synthesized complexes have been evaluated for their thermal degradation studies using TG-DTA analytical methods in static air. Thermodynamic and kinetic parameters were evaluated from the TG-DTA curves using Arrhenius equation.
Keywords: Schiff base / Tg Dta / kinetic / HLA / Thermodynamic / NMR spectroscopy / Arrhenius equation / Thermal degradation

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