Small- and Wide-Angle X-Ray Scattering (SAXS/WAXS) with Temperature-Controlled Stages Makes Phase Identification Faster than Ever
- 1 November 2021
- journal article
- materials applications
- Published by Oxford University Press (OUP) in Microscopy Today
- Vol. 29 (6), 30-36
- https://doi.org/10.1017/s1551929521001358
Abstract
X-ray diffraction (XRD) is a fingerprint technique for the analysis of atomic and molecular structures of crystalline materials, from polymers and plastics, through to structural composites and biomaterials. These all have crystallographic phases in the nanostructure, which greatly influence the macro properties of the material—from insulin and hemoglobin to semiconductors and solar cells. Here, we look at how XRD analysis using a small- and wide-angle X-ray scattering (SAXS/WAXS) system under full vacuum brings the possibility of crystallographic sample characterization, with temperature and environmental control, direct to the laboratory, and how this improves the workflow for phase identification.Keywords
This publication has 3 references indexed in Scilit:
- Small-Angle X-Ray Scattering from RNA, Proteins, and Protein ComplexesAnnual Review of Biophysics and Biophysical Chemistry, 2007
- l -Pyroglutamate Spontaneously Formed from l -Glutamate Inhibits Growth of the Hyperthermophilic Archaeon Sulfolobus solfataricusApplied and Environmental Microbiology, 2001
- Small-Angle X-ray Scattering of PolymersChemical Reviews, 2001