Application of Single Scan Differential Scanning Calorimetry Technique for Determination of Kinetic Parameters of Crystallisation in Se-Sb-Ag
Published: 1 January 2019
Journal of Crystallization Process and Technology
,
Volume 09,
pp 1-11; https://doi.org/10.4236/jcpt.2019.91001
Abstract: A single scan has been performed in Differential Scanning Calorimetry (DSC) at a heating rate of 15oC/min under non-isothermal conditions to investigate the crystallization kinetics of glassy Se90Sb10-xAgx alloys (where x = 2, 4, 6, 8). For this purpose, Handerson’s theory based on non-isothermal method for thermal analysis of single-scan DSC data has been used. The activation energy of crystallization and order parameter has been determined and composition dependence of these parameters has been discussed.
Keywords: Differential Scanning Calorimetry / Crystallization / Order Parameter
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