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Validation of analysis method for determining ketoprofen concentration in pharmaceutical dosage form using high performance liquid chromatography

Tadjuddin Naid, Wahyu Rizandi Syukur, Amran Ilyas, Seniwati Dali, Baharuddin Hamzah
European Journal of Chemistry , Volume 4, pp 58-60; doi:10.5155/eurjchem.4.1.58-60.678

Abstract: The study was conducted with the purpose to develop and validate a high performance liquid chromatography method with UV detector to determine ketoprofen content in tablet preparation using ethanol-phosphate buffer (pH = 6.0, 80:20, v:v). The method was validated toward parameters of accuracy, precision, linearity, selectivity, LOD and LOQ. The results obtained fulfill the validation requirement of the ketoprofen tablet in the form of LOD = 0.5302 ppm and LOQ = 1.7676 ppm.
Keywords: tablet / ethanol / Determining Ketoprofen / high performance liquid chromatography / Ketoprofen Concentration / Loq

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